Proceedings of the Estonian Academy of Sciences, Chemistry |
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3C NMR a-hydroxylation acetate Akadeemia tee 15 alcohols 4a asymmetric synthesis Baeyer-Villiger oxidation bimorpholine capillary catalyst CH2N Chem Chemical Physics chiral ligands chromatography on silica column chromatography compounds crude product cyclic database dienolate Ehitajate tee electrophoretic enantiomeric enantioselectivity enolates enone ester Estonian Estonian Acad Estonian Academy Publishers Et3N ethyl full-generation H NMR CDC13 half-generations head-list HPLC hydrogen acids hydroxyl Institute of Chemical Institute of Chemistry Kanger ketones lactones LINCS code Margus LOPP menu MeOH methanol MgSO4 mixture was stirred mmol obtained organic chemistry oxidation of cyclobutanones oxidation of ketones Paju poly(amidoamine prochiral purified r-BuCHO r-BuOOH reaction mixture retrieval ring cleavage room temperature Scheme Screen-image Sharpless Sharpless-Katsuki complex SiCH3 silica gel solution solvent structure substrate synthesis Table Tallinn Technical University tartaric acid Tartu tetraester Tetrahedron Tomalia Tonis PEHK triester Ulo Lille University of Tartu Viktor Palm yield